2-Bromopropane → HCID 18507612, compound

HRID 1355721Notes

Reaction equation

HRID 1355721 reaction equation
[NH2:1][C:2]1[NH:3][C:4](=[S:16])[C:5]([C:14]#[N:15])=[C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:7]=1.[CH:17](Br)([CH3:19])[CH3:18].CC[O-].[Na+]>C(O)C>[NH2:1][C:2]1[N:3]=[C:4]([S:16][CH:17]([CH3:19])[CH3:18])[C:5]([C:14]#[N:15])=[C:6]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=2)[N:7]=1

Participants

5

Reactant 3

HCID 63582-BromopropaneHCID 2723922Sodium ethoxideHCID 178509378HCID 178509378, compound

Product 1

HCID 18507612HCID 18507612, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

From 2-amino-4-phenyl-6-thioxo-1,6-dihydro-pyrimidine-5-carbonitrile, isopropyl bromide and sodium ethylate in ethanol. EI-MS m/e (%): 270 (M+, 30), 269 ([M—H]+, 100).

Sources & evidence

ORD record
ord-2f0c0dacb87747ac8bc86ae8d175ba56
Source dataset
uspto-grants-2003_07
Patent number
US06586441B2

Reaction notes

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