1-Butanol → HCID 86583752, compound

HRID 1355936Notes

Reaction equation

HRID 1355936 reaction equation

[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6]1[C:11]([I:12])=[C:10](S(C)=O)[N:9]=[C:8]([NH2:16])[N:7]=1.[CH2:17]([OH:21])[CH2:18][CH2:19][CH3:20].C1CCN2C(=NCCC2)CC1>C1COCC1>[CH2:17]([O:21][C:10]1[C:11]([I:12])=[C:6]([C:2]2[O:1][CH:5]=[CH:4][CH:3]=2)[N:7]=[C:8]([NH2:16])[N:9]=1)[CH2:18][CH2:19][CH3:20]

Participants

5

Reactant 3

HCID 2631-Butanol

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-ene

HCID 18507211HCID 18507211, compound

Product 1

HCID 86583752HCID 86583752, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

From 4-furan-2-yl-5-iodo-6-methanesulfinyl-pyrimidin-2-yl-amine, butanol and DBU in THF. ES-MS m/e (%): 360 (M+H+, 100).

Sources & evidence

ORD record: ord-4ed365f92ff540819d05962987703af4
Source dataset: uspto-grants-2003_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06586441B2

Reaction notes

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