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HRID1360379

反应详情

EQUATION

反应方程式

HRID 1360379 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CC(C)=CCBr
HCID70092

2-Butene, 1-bromo-3-methyl-

C5H9Br

结构：Cn1c(=O)[nH]c(=O)c2[nH]c(Br)nc21
HCID1548797

8-Bromo-3-methyl-1H-purine-2,6(3H,7H)-dione

C6H5BrN4O2

PRODUCTS

生成物

1
结构：CC(C)=CCn1c(Br)nc2c1c(=O)[nH]c(=O)n2C
HCID3435331

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

50 g of 8-bromo-3-methyl-3,7-dihydropurine-2,6-dione are introduced into 900 ml of DMF, and 14.1 g of potassium carbonate are added. The suspension is heated to an internal temperature of 60° C., and 31.7 g of 1-bromo-3-methyl-2-butene are slowly 10 added. The mixture is stirred at this temperature for 3 hours and then 1.2 1 of water are added. The solid is filtered off with suction, thoroughly washed with water and dried in vacuo at 45° C.

WORKUP

后处理

  1. additionare added
  2. additionadded
  3. filtrationThe solid is filtered off with suction
  4. washthoroughly washed with water
  5. customdried in vacuo at 45° C.