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HRID1360653

反应详情

EQUATION

反应方程式

HRID 1360653 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(Cl)c1cc(F)c(F)cc1F
HCID145164

2,4,5-Trifluorobenzoyl chloride

C7H2ClF3O

结构：CCOC(=O)C=C(C)NC1CCCC1
HCID66962611

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(C(=O)c1cc(F)c(F)cc1F)=C(C)NC1CCCC1
HCID178472172

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

CONDITIONS

反应条件

温度
65 °C

PROCEDURE

实验过程

Under ice cooling, triethylamine and 2,4,5-trifluorobenzoyl chloride were added to a solution of ethyl 3-(cyclopentylamino)buta-2-enoate in dioxane, for stirring at ambient temperature for 30 minutes and at 65° C. for one hour, to obtain ethyl 3-(cyclopentylamino)-2-(2,4,5-trifluorobenzoyl)buta-2-enoate.