Methyl Methacrylate → HCID 23569822, compound

HRID 1363322Notes

Reaction equation

[N:1]([CH2:8][CH2:9][OH:10])([CH2:5][CH2:6][OH:7])[CH2:2][CH2:3][OH:4].[C:11](OC)(=[O:15])[C:12]([CH3:14])=[CH2:13].C[O-].[Na+]>>[C:11]([O:4][CH2:3][CH2:2][N:1]([CH2:8][CH2:9][OH:10])[CH2:5][CH2:6][OH:7])(=[O:15])[C:12]([CH3:14])=[CH2:13]

Participants

Reactant 3

HCID 6658Methyl Methacrylate

HCID 7618Triethanolamine

HCID 10942334Sodium Methoxide

Product 1

HCID 23569822HCID 23569822, compound

Procedure

Triethanolamine is reacted with methyl methacrylate and sodium methoxide at ambient temperature until the unreacted mono-, di- and trimethacryloxy substituted products reached the desired distribution as determined by gas chromatography. The resulting solution is stripped of excess reagent under reduced pressure. Next, N-(2-methacryloxyethyl)diethanolamine is separated from the solution by chromatography.

Workup

customNext, N-(2-methacryloxyethyl)diethanolamine is separated from the solution by chromatography

Sources & evidence

ORD record: ord-5d49b672a835469db8b543ff4eb53acc
Source dataset: uspto-grants-2011_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07884141B2

Reaction notes

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