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HRID1368316

反应详情

EQUATION

反应方程式

HRID 1368316 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：COc1ccc(Cc2nnc(C(C)NC(=O)C(C)(CCCc3ccccc3)C(C)=O)c(=O)[nH]2)cc1OC
HCID136017769

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(Cc2nn3c(C(C)(CCCc4ccccc4)C(C)=O)nc(C)c3c(=O)[nH]2)cc1OC
HCID135528458

未命名化合物

PROCEDURE

实验过程

Analogously to Example 1, 3.08 g (6.07 mmol) of 2-acetyl-N-{1-[3-(3,4-dimethoxybenzyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]ethyl}-2-methyl-5-phenylpentanamide and 4.44 mg (29.0 mmol) of phosphorus oxychloride are reacted to give 7-(1-acetyl-1-methyl-4-phenylbutyl)-2-(3,4-dimethoxybenzyl)-5-methylimidazo[5,1-f][1,2,4]-triazin-4(3H)-one.