huagongshe.com
HRID1368912

反应详情

EQUATION

反应方程式

HRID 1368912 的结构方程式

REACTANTS

反应物

1
结构：O=C(O)C[C@H](NC(=O)Cc1ccccc1)c1cccc([N+](=O)[O-])c1
HCID711905

未命名化合物

PRODUCTS

生成物

1
结构：N[C@@H](CC(=O)O)c1cccc([N+](=O)[O-])c1
HCID706689

(s)-3-amino-3-(3-nitrophenyl)propionic acid

C9H10N2O4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

(S)-3-(3-nitrophenyl)-3-phenylacetylaminopropionic acid is treated with 10 ml of 6N HCl solution. (S)-3-amino-3-(3-nitrophenyl)propionic acid is obtained and is reacted further in analogy to the R enantiomer. This gives (S)-3-{2-[4-(4-methylpyridin-2-ylamino)butyrylamino]acetylamino}-3-(3-nitrophenyl)propionic acid, (S)-3-{2-[4-(4-methylpyridin-2-ylamino)butyrylamino]acetylamino}-3-(3-nitrophenyl propionic acid sodium salt, (S)-3-{2-[4-(4-methylpyridin-2-ylamino)butyrylamino]acetylamino}-3-(3-nitrophenyl)propionic acid trifluoroacetate, RT* 16.89 min, FAB-MS (M+H)+ 444.