Methyl Chloride → Stearoxypropyltrimonium chloride

HRID 1369264Notes

Reaction equation

HRID 1369264 reaction equation
[CH3:1][N:2]([CH2:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])[CH3:3].[CH3:26][Cl:27]>C(O)(C)C>[Cl-:27].[CH3:1][N+:2]([CH2:4][CH2:5][CH2:6][O:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH3:25])([CH3:26])[CH3:3]

Participants

4

Reactant 2

HCID 6327Methyl Chloride2×HCID 87142Stearoxypropyl dimethylamine

Product 1

HCID 18519353Stearoxypropyltrimonium chloride

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent2×

Procedure

A 1-L autoclave equipped with a stirrer and a thermometer was charged with N,N-dimethyl-3-octadecyloxy-propylamine (300 g) obtained in Example 1A, isopropyl alcohol (90 g) and methyl chloride (100 g) to conduct a reaction at 90° C. for 6 hours. Excessive methyl chloride was topped to obtain an isopropyl alcohol solution of N,N,N-trimethyl-3-octadecyloxypropylammonium chloride. The quaternizing rate was 98% (KSTM 20082).

Workup

  1. customA 1-L autoclave equipped with a stirrer
  2. customa reaction at 90° C. for 6 hours

Sources & evidence

ORD record
ord-097b88ca3b70447297adf96da3cff418
Source dataset
uspto-grants-2003_06
Patent number
US06576794B2

Reaction notes

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