huagongshe.com
HRID1374609

反应详情

EQUATION

反应方程式

HRID 1374609 的结构方程式

REACTANTS

反应物

5
结构：CN1CCOCC1
HCID7972

4-Methylmorpholine

C5H11NO

结构：CNCC(=O)OC
HCID83545

Methyl N-methylglycinate

C4H9NO2

结构：CN(C)[P+](On1nnc2ccccc21)(N(C)C)N(C)C.F[P-](F)(F)(F)(F)F
HCID151348

Tri(dimethylamino)benzotriazol-1-yloxyphosphonium hexafluorophosphate

C12H22F6N6OP2

结构：CN(C)C=O.Cc1ccc(S(=O)(=O)N(C)CC(=O)O)cc1
HCID86589137

未命名化合物

结构：COC(=O)[C@H](Cc1c[nH]cn1)NCc1ccccc1
HCID178501396

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)CN(C)S(=O)(=O)c1ccc(C)cc1
HCID3277444

未命名化合物

PROCEDURE

实验过程

N-(Toluene-4-sulfonyl)sarcosine methyl ester was prepared from sarcosine methyl ester using the procedure described in Method 1. The title compound was prepared by coupling in DMF N-(toluene-4-sulfonyl)sarcosine with (N-benzyl)histidine methyl ester in the presence of BOP and NMM, to give after aqueous workup and flash chromatography, the title compound.

WORKUP

后处理

  1. customThe title compound was prepared
  2. customto give after aqueous workup and flash chromatography