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HRID1375355

反应详情

EQUATION

反应方程式

HRID 1375355 的结构方程式

REACTANTS

反应物

1
结构：CC(C)(C)OC(=O)CN1C(=O)CC(=O)N(c2ccccc2)c2ccccc21
HCID86602389

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)CN1C(=O)CC(=O)N(c2ccccc2)c2ccccc21
HCID69427552

未命名化合物

收率 97%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

tert-butyl (2,4-dioxo-5-phenyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)acetate (9.5 g, 25.9 mM) was dissolved in 200 ml of 4N HCl in dioxane and stirred overnight. Solvent was evaporated under reduced pressure providing 7.8 g of product.

WORKUP

后处理

  1. customSolvent was evaporated under reduced pressure