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HRID1376065

反应详情

EQUATION

反应方程式

HRID 1376065 的结构方程式

REACTANTS

反应物

3
结构：C[Si](C)(C)C#N
HCID82115

Silanecarbonitrile, trimethyl-

C4H9NSi

结构：CC(C)(C)OC(=O)N1CCNCC1
HCID143452

tert-Butyl piperazine-1-carboxylate

C9H18N2O2

结构：O=CCC1CCCCC1
HCID316627

2-cyclohexylacetaldehyde

C8H14O

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCN(C(C#N)CC2CCCCC2)CC1
HCID58786388

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of cyclohexaneacetaldehyde (8.45 g, 66.96 mmol) and TMSCN (17.9 mL, 133.92 mmol) in MeOH was stirred for 2 h at 23° C. and N-BOC-piperazine (13.72 g, 73.66 mmol) was added. After 24 the solvent was evaporated to give the title compound.

WORKUP

后处理

  1. customAfter 24 the solvent was evaporated