反应详情

Triethylamine (2 moles) was added to a solution of the product from step (a) (1 mole) in toluene. When addition was complete, benzaldehyde (1 mole) was added. The mixture was azeotroped until no further water was collected, then cooled to room temperature and filtered. The filtrate was evaporated in vacuo to give the desired product as an oil.

1. additionWhen addition
2. customThe mixture was azeotroped until no further water
3. customwas collected
4. filtrationfiltered
5. customThe filtrate was evaporated in vacuo