HRID1378893

反应详情

EQUATION

反应方程式

HRID 1378893 的结构方程式

PROCEDURE

实验过程

Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89°-90° C./2 mmHg.

WORKUP

后处理

  1. customas described in Synthesis Example 1, (1),
  2. distillationthe crude oil (24 g) was purified by distillation under reduced pressure