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HRID1380088

反应详情

EQUATION

反应方程式

HRID 1380088 的结构方程式

REACTANTS

反应物

3
结构：BrCc1ccccc1
HCID7498

alpha-Bromotoluene

C7H7Br

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)Cc1ccc(O)c(Cl)c1
HCID92625

Methyl 3-chloro-4-hydroxyphenylacetate

C9H9ClO3

PRODUCTS

生成物

1
结构：COC(=O)Cc1ccc(OCc2ccccc2)c(Cl)c1
HCID561937

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

A mixture of 8.7 g (43.4 mmoles) of methyl 3-chloro-4-hydroxyphenylacetate, 6.2 g (44.8 mmoles) of powdered anhydrous potassium carbonate, 7.6 g (44.6 mmoles) of benzyl bromide, and 25 ml of methyl ethyl ketone was refluxed for six hours.

WORKUP

后处理

  1. temperaturewas refluxed for six hours