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HRID1381493

反应详情

EQUATION

反应方程式

HRID 1381493 的结构方程式

REACTANTS

反应物

3
结构：ClCCCBr
HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

结构：[Na]
HCID5360545

Sodium

Na

结构：O=C1COc2cc(O)ccc2N1
HCID10057870

7-hydroxy-2H-benzo[b][1,4]oxazin-3(4H)-one

C8H7NO3

PRODUCTS

生成物

1
结构：O=C1COc2cc(OCCCCl)ccc2N1
HCID13343872

未命名化合物

收率 65%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCCO
溶剂HCID8076

2-Ethoxyethanol

C4H10O2

PROCEDURE

实验过程

7-Hydroxy-2H-1,4-benzoxazin-3(4H)-one was treated with 3-bromo-1-chloro-propane and sodium metal in ethyleneglycol monoethyl ether to give the desired product in 65% yield, mp 95° C.