HRID1381849

反应详情

EQUATION

反应方程式

HRID 1381849 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The copper, barium, and yttrium solutions were mixed and the potassium oxalate solution was added all at once with vigorous stirring. The pH of the solution was 11.3. A brown gelatinous precipitate formed, and it was filtered, washed thoroughly with water, dried at 120° C., and crushed to a fine powder. The elemental analysis shown in the table below suggested YBa2Cu3 (OH)3 (Ox)2O3.H2O.

WORKUP

后处理

  1. customA brown gelatinous precipitate formed
  2. filtrationit was filtered
  3. washwashed thoroughly with water
  4. customdried at 120° C.
  5. customcrushed to a fine powder