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HRID1381966

反应详情

EQUATION

反应方程式

HRID 1381966 的结构方程式

REACTANTS

反应物

4
结构：[I-].[Na+]
HCID5238

Sodium Iodide

INa

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：O=C([O-])[O-].[Na+].[Na+]
HCID10340

Carbonic acid sodium salt (1:2)

CNa2O3

结构：O=C1c2ccccc2C(=O)N1OCCBr
HCID199875

1H-Isoindole-1,3(2H)-dione, 2-(2-bromoethoxy)-

C10H8BrNO3

PRODUCTS

生成物

1
结构：O=C1c2ccccc2C(=O)N1OCCN1CCCCC1
HCID13983476

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCC(C)=O
溶剂HCID6569

Methyl ethyl ketone

C4H8O

PROCEDURE

实验过程

21.3 g (0.25 mol) of piperidine are added to a solution of 54 g (0.2 mol) of N-(2-bromoethoxy)phthalimide in 800 ml of methyl ethyl ketone, in the presence of 31.5 g (0.3 mol) of sodium carbonate and 1 g of sodium iodide.