Triethylamine → HCID 18672830, compound

HRID 1385496Notes

Reaction equation

HRID 1385496 reaction equation
[F:1][C:2]([F:28])([F:27])[C:3]1[CH:26]=[CH:25][C:6]2=[N:7][N:8]([C:10]3[CH:15]=[C:14]([CH2:16][CH2:17][CH2:18][NH2:19])[CH:13]=[C:12]([C:20]([CH3:23])([CH3:22])[CH3:21])[C:11]=3[OH:24])[N:9]=[C:5]2[CH:4]=1.[C:29](Cl)(=[O:33])[C:30]([CH3:32])=[CH2:31].C(N(CC)CC)C>C1(C)C=CC=CC=1>[F:28][C:2]([F:1])([F:27])[C:3]1[CH:26]=[CH:25][C:6]2=[N:7][N:8]([C:10]3[CH:15]=[C:14]([CH2:16][CH2:17][CH2:18][NH:19][C:29](=[O:33])[C:30]([CH3:32])=[CH2:31])[CH:13]=[C:12]([C:20]([CH3:22])([CH3:23])[CH3:21])[C:11]=3[OH:24])[N:9]=[C:5]2[CH:4]=1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 13528Methacryloyl chlorideHCID 18672840HCID 18672840, compound

Product 1

HCID 18672830HCID 18672830, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The title compound is prepared by the reaction of the compound of Example 58 with methacryloyl chloride in the presence of triethylamine in toluene.

Sources & evidence

ORD record
ord-0600f6c7501b48058b868ce9992bca85
Source dataset
uspto-grants-2001_07
Patent number
US06262151B1

Reaction notes

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