反应详情

In 300 ml of toluene, 83.1 g (0.5 mol) of p-cyclohexylphenol was dissolved, and then 150 g of 2-chloroethyl vinyl ether, 25 g of sodium hydroxide, 5 g of tetrabutylammonium bromide and 60 g of triethylamine were added thereto, followed by a reaction at 120° C. for 5 hours. The reaction solution was washed with water, and excess chloroethyl vinyl ether and toluene were removed by distillation. The resulting oil was purified by distillation under reduced pressure to obtain 4-cyclohexylphenoxyethyl vinyl ether.

1. customfollowed by a reaction at 120° C. for 5 hours
2. washThe reaction solution was washed with water, and excess chloroethyl vinyl ether and toluene
3. customwere removed by distillation
4. distillationThe resulting oil was purified by distillation under reduced pressure