Ethyl Acrylate → HCID 12375248, compound

HRID 1385990Notes

Reaction equation

HRID 1385990 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[C:4]([CH3:9])[CH:3]=1.[Na].[C:11]([O:15][CH2:16][CH3:17])(=[O:14])[CH:12]=[CH2:13]>C(O)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([O:8][CH2:13][CH2:12][C:11]([O:15][CH2:16][CH3:17])=[O:14])=[C:4]([CH3:9])[CH:3]=1

Participants

5

Reactant 3

HCID 8821Ethyl AcrylateHCID 148554-Chloro-2-methylphenolHCID 5360545Sodium

Product 1

HCID 12375248HCID 12375248, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The sub-title compound was prepared according to the method described in Example 27(i) above from 4-chloro-2-methylphenol (4.99 g; 35.0 mmol), sodium (0.055 g; 2.4 mmol), ethanol (1.5 mL) and ethyl acrylate (4.1 g; 41 mmol). The crude product (1.98 g; 23%) was used for the next step without further purification.

Workup

  1. customThe crude product (1.98 g; 23%) was used for the next step without further purification

Sources & evidence

ORD record
ord-63967bfe95ad4f41a2caa3d899950b4b
Source dataset
uspto-grants-2001_07
Patent number
US06265397B1

Reaction notes

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