Cyanuric chloride → HCID 21182127, compound

HRID 1386508Notes

Reaction equation

HRID 1386508 reaction equation
[CH3:1][O:2][N:3]1[C:8]([CH3:10])([CH3:9])[CH2:7][CH:6]([CH2:11][CH2:12][CH2:13][CH2:14][NH2:15])[CH2:5][C:4]1([CH3:17])[CH3:16].[N:18]1[C:25]([Cl:26])=[N:24][C:22](Cl)=[N:21][C:19]=1[Cl:20].[OH-].[Na+]>C1(C)C(C)=CC=CC=1.O>[Cl:20][C:19]1[N:18]=[C:25]([Cl:26])[N:24]=[C:22]([NH:15][CH2:14][CH2:13][CH2:12][CH2:11][CH:6]2[CH2:7][C:8]([CH3:10])([CH3:9])[N:3]([O:2][CH3:1])[C:4]([CH3:17])([CH3:16])[CH2:5]2)[N:21]=1

Participants

6

Reactant 3

HCID 7954Cyanuric chlorideHCID 14798Sodium HydroxideHCID 70247675HCID 70247675, compound

Product 1

HCID 21182127HCID 21182127, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 7237O-XyleneSolvent

Procedure

39.7 g (163 mmoles) of N-(1-methoxy-2,2,6,6-tetramethyl-4-piperidyl)butylamine are slowly added to a solution of 30 g (163 mmoles) of cyanuric chloride in 180 ml of xylene, maintained at room temperature. After the addition, the mixture is stirred for ½ hour at room temperature and subsequently, a solution of 6.8 g (170 mmoles) of sodium hydroxide in 45 ml of water is slowly added, maintaining the temperature at room temperature.

Workup

  1. additionAfter the addition
  2. temperaturemaintaining the temperature at room temperature

Sources & evidence

ORD record
ord-2bcdd30447704c26926d40e0c6b8bf2b
Source dataset
uspto-grants-2001_07
Patent number
US06265473B1

Reaction notes

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