Allylamine → HCID 86737434, compound

HRID 1389521Notes

Reaction equation

HRID 1389521 reaction equation
[CH2:1]([NH2:4])[CH:2]=[CH2:3].[CH2:5]1[S:10](=[O:12])(=[O:11])[O:9][CH2:8][CH2:7][CH2:6]1>CO>[CH2:1]([NH:4][CH:5]([S:10]([OH:12])(=[O:11])=[O:9])[CH2:6][CH2:7][CH3:8])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 7853AllylamineHCID 154111,4-Butane sultone

Product 1

HCID 86737434HCID 86737434, compoundYield 36.3%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

A solution of 57 g of allylamine and 136 g of butanesultone in 1 l of methanol was stirred a room temperature for 48 h. After evaporation, washing of the residue with ether and drying under vacuum, 70 g of N-allyl-aminobutane sulphonic acid were obtained.

Workup

  1. customAfter evaporation
  2. washwashing of the residue with ether
  3. customdrying under vacuum

Sources & evidence

ORD record
ord-d8e11faaaccc4257b3e9034802d91093
Source dataset
uspto-grants-1981_01
Patent number
US04245036

Reaction notes

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