Styrene Oxide → HCID 13210715, compound

HRID 1389553Notes

Reaction equation

[CH3:1][O:2][CH2:3][CH2:4][NH2:5].[CH2:6]1[O:14][CH:7]1[C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[OH:14][CH:7]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:6][NH:5][CH2:4][CH2:3][O:2][CH3:1]

Participants

Reactant 2

HCID 7276Styrene Oxide

HCID 80182-Methoxyethylamine

Product 1

HCID 13210715HCID 13210715, compound

Procedure

To 157 g of refluxing 2-methoxyethylamine is added dropwise 25 g styrene oxide during a period of 15 minutes. After addition of the amine, the mixture is allowed to reflux for another two hours.

Workup

temperatureto reflux for another two hours

Sources & evidence

ORD record: ord-105b201f6a7344e5b8ca980d97d31c8f
Source dataset: uspto-grants-1981_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04245103

Reaction notes

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