Furfural → HCID 20456642, compound

HRID 1389722Notes

Reaction equation

HRID 1389722 reaction equation
[CH:1](=O)[C:2]1[O:6][CH:5]=[CH:4][CH:3]=1.[CH:8]1[CH2:12][CH:11]=[CH:10][CH:9]=1>C(NCC)C.CO>[O:6]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:1]1[C:9](=[CH2:10])[CH:8]=[CH:12][CH:11]=1

Participants

5

Reactant 2

HCID 7362FurfuralHCID 7612Cyclopentadiene

Product 1

HCID 20456642HCID 20456642, compound

Reagents, catalysts & solvents 2

HCID 8021DiethylamineCatalystHCID 887MethanolSolvent

Procedure

About equal molar amounts of furfural and cyclopentadiene are reacted in the presence of diethylamine catalyst and about 33% methanol solvent according to the method suggested by C. Schmidt, Chem, Ber., Volume 90, p. 1352, 1957. A viscous dark material is separated from the water layer.

Workup

  1. customA viscous dark material is separated from the water layer

Sources & evidence

ORD record
ord-306bd05b3e0b44d3979410885d4b2c1a
Source dataset
uspto-grants-1981_01
Patent number
US04246167

Reaction notes

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