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HRID1390426

反应详情

EQUATION

反应方程式

HRID 1390426 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CNC(CO)(CO)CO
HCID10164823

未命名化合物

结构：COC(=O)c1ccc([N+](=O)[O-])cc1C(=O)Cl
HCID13221842

Methyl 2-(chlorocarbonyl)-4-nitrobenzoate

C9H6ClNO5

PRODUCTS

生成物

1
结构：COC(=O)c1cc(C(=O)N(C)C(CO)(CO)CO)cc([N+](=O)[O-])c1
HCID22749370

未命名化合物

PROCEDURE

实验过程

Methoxy-carbonyl-5-nitrobenzoyl chloride [G. B. Hoey, et al., J. Med. Chem., 6, 24 (1963)] is added to a cold stirred slurry of N-methyl-tris(hydroxymethyl)-methylamine and potassium carbonate in dimethylformamide to form a solution of N-methyl-5-nitro-N-[tris(hydroxymethyl)methyl]isophthalamic acid, methyl ester.