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HRID1393867

反应详情

EQUATION

反应方程式

HRID 1393867 的结构方程式

REACTANTS

反应物

3
结构：COc1ccc(S(=O)(=O)Cl)cc1
HCID7401

4-Methoxybenzenesulphonyl chloride

C7H7ClO3S

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC(C)[C@H](N)C(=O)OC(C)(C)C.Cl
HCID12490702

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccc(S(=O)(=O)NC(C(=O)OC(C)(C)C)C(C)C)cc1
HCID10783604

N-[(4-Methoxyphenyl)sulfonyl]valine 1,1-dimethylethyl ester

C16H25NO5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Valine tert-butyl ester hydrochloride is reacted with 4-methoxybenzenesulfonyl chloride in dichloromethane in the presence of triethylamine, to give tert-butyl 2-{[(4-methoxyphenyl)sulfonyl]amino}-3-methylbutanoate.