Benzoic Acid → HCID 59681881, compound

HRID 1394165Notes

Reaction equation

HRID 1394165 reaction equation
[CH:1]([C:3]1[CH:4]=[C:5]([C:9]2[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=2[O:15][C:16]([F:19])([F:18])[F:17])[CH:6]=[CH:7][CH:8]=1)=O.[O:20]1[CH2:24][C:23](=[O:25])[NH:22][C:21]1=[O:26].N1CCCCC1.C(O)(=O)C1C=CC=CC=1>C1(C)C=CC=CC=1>[F:17][C:16]([F:19])([F:18])[O:15][C:10]1[CH:11]=[CH:12][CH:13]=[CH:14][C:9]=1[C:5]1[CH:6]=[CH:7][CH:8]=[C:3](/[CH:1]=[C:24]2/[C:23](=[O:25])[NH:22][C:21](=[O:26])[O:20]/2)[CH:4]=1

Participants

6

Reactant 4

HCID 243Benzoic AcidHCID 8082PiperidineHCID 973892,4-OxazolidinedioneHCID 16768574HCID 16768574, compound

Product 1

HCID 59681881HCID 59681881, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The title compound was prepared by reacting 3-formyl-(2′-trifluoromethoxy-1,1′-biphenyl) (from Example 56, Step A) with 2,4-oxazolidinedione in toluene in the presence of piperidine and benzoic acid as described in Example 56, Step B.

Sources & evidence

ORD record
ord-c67abbef2f3b4bf892cf333d9ca8be23
Source dataset
uspto-grants-2008_03
Patent number
US07348348B2

Reaction notes

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