Sodium Iodide → HCID 53473125, compound

HRID 1401358Notes

Reaction equation

HRID 1401358 reaction equation
CS(O[CH2:6][CH2:7][C:8]1[N:9]=[N:10][N:11]([C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:12]=1)(=O)=O.C(N(CC)CC)C.[I-].[Na+]>>[C:13]1([N:11]2[CH:12]=[C:8]([CH:7]=[CH2:6])[N:9]=[N:10]2)[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1

Participants

4

Reactant 3

HCID 5238Sodium IodideHCID 8471TriethylamineHCID 117722862HCID 117722862, compound

Product 1

HCID 53473125HCID 53473125, compound

Procedure

2-(1-phenyl-1H-1,2,3-triazol-4-yl)ethyl methanesulfonate (1.43 g, 5.35 mmol), triethylamine (1.62 g, 16.05 mmol) and sodium iodide (2.41 g, 16.05 mmol) were added to a vial to produce 1-phenyl-4-vinyl-1H-1,2,3-triazole.

Sources & evidence

ORD record
ord-110691b52c994cfb87f8b63cc13c76da
Source dataset
uspto-grants-2014_12
Patent number
US08907105B1

Reaction notes

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