Diisopropylcarbodiimide → HCID 178468681, compound

HRID 1406436Notes

Reaction equation

HRID 1406436 reaction equation
[CH2:1]([O:3][C:4](=[O:13])[C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[C:7]([NH2:12])[CH:6]=1)[CH3:2].[Cl:14][C:15]1[CH:20]=[CH:19][CH:18]=[C:17]([Cl:21])[C:16]=1[N:22]=[C:23]=S.CC(C)N=C=NC(C)C>CN(C=O)C>[CH2:1]([O:3][C:4]([C:5]1[CH:10]=[CH:9][C:8]2[NH:11][C:23]([NH:22][C:16]3[C:15]([Cl:14])=[CH:20][CH:19]=[CH:18][C:17]=3[Cl:21])=[N:12][C:7]=2[CH:6]=1)=[O:13])[CH3:2]

Participants

5

Reactant 3

HCID 12734DiisopropylcarbodiimideHCID 1232391,3-Dichloro-2-isothiocyanatobenzeneHCID 458855Ethyl 3,4-Diaminobenzoate

Product 1

HCID 178468681HCID 178468681, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared analogously to example 1c from 3,4-diamino-benzoic acid ethyl ester and 1,3-dichloro-2-thioisocyanato-benzene with DIC in DMF.

Sources & evidence

ORD record
ord-a71578322c57480eb1d3288183cda6fd
Source dataset
uspto-grants-2014_12
Patent number
US08916599B2

Reaction notes

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