Cyanuric chloride → HCID 58507984, compound

HRID 1408454Notes

Reaction equation

HRID 1408454 reaction equation
Cl[C:2]1[N:7]=[C:6]([Cl:8])[N:5]=[C:4]([Cl:9])[N:3]=1.[NH2:10][CH2:11][CH2:12][N:13]1[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]1>>[Cl:9][C:4]1[N:5]=[C:6]([Cl:8])[N:7]=[C:2]([NH:10][CH2:11][CH2:12][N:13]2[CH2:18][CH2:17][CH2:16][CH2:15][CH2:14]2)[N:3]=1

Participants

3

Procedure

Following the general procedure A, 2,4,6-trichloro-1,3,5-triazine was coupled with 1-(2-Aminoethyl)piperidine with reaction time of 2 h. Purification by column chromatography gave the title compound.

Workup

  1. customPurification by column chromatography

Sources & evidence

ORD record
ord-7ec77d0bd0b542e798eb933dfd4e5b14
Source dataset
uspto-grants-2014_12
Patent number
US08921361B2

Reaction notes

Loading…