2-Isothiocyanato-6-methylheptane → HCID 178443610, compound

HRID 1419754Notes

Reaction equation

HRID 1419754 reaction equation
Cl.[NH2:2][C:3]1[CH:7]=[C:6]([Cl:8])[S:5][C:4]=1[S:9]([NH2:12])(=[O:11])=[O:10].[CH3:13][CH:14]([N:21]=[C:22]=S)[CH2:15][CH2:16][CH2:17][CH:18]([CH3:20])[CH3:19]>C(OCC)(=O)C>[Cl:8][C:6]1[S:5][C:4]2[S:9](=[O:10])(=[O:11])[N:12]=[C:22]([NH:21][CH:14]([CH3:13])[CH2:15][CH2:16][CH2:17][CH:18]([CH3:20])[CH3:19])[NH:2][C:3]=2[CH:7]=1

Participants

4

Reactant 2

HCID 27598522-Isothiocyanato-6-methylheptaneHCID 688206263-Amino-5-chlorothiophene-2-sulfonamide hydrochloride

Product 1

HCID 178443610HCID 178443610, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and 1,5-dimethylhexyl isothiocyanate by a procedure analogous to the procedure described in example 3Bc-d; mp 197°-199° C. (ethyl acetate); 1H-NMR (DMSO-d6): δ 0.85 (d, 6H), 1.12 (d, 3H), 1.1-1.6 (m, 7H), 3.77 (m, 1H), 7.07 (s, 1H), 7.12 (br. s, 1H), 10.72 (br. s, 1H).

Sources & evidence

ORD record
ord-dd8a63192642429ebcfff7020b1dc6e9
Source dataset
uspto-grants-1999_03
Patent number
US05889002

Reaction notes

Loading…