Methacrylic Acid → HCID 18364573, compound

HRID 1420484Notes

Reaction equation

HRID 1420484 reaction equation
[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([OH:23])(=[O:22])[C:19]([CH3:21])=[CH2:20]>O1CCCC1>[C:1]([O:6][CH3:7])(=[O:5])[C:2]([CH3:4])=[CH2:3].[C:8]([O:13][C:14]([CH3:17])([CH3:16])[CH3:15])(=[O:12])[C:9]([CH3:11])=[CH2:10].[C:18]([OH:23])(=[O:22])[C:19]([CH3:21])=[CH2:20]

Participants

5

Reactant 3

HCID 4093Methacrylic AcidHCID 6658Methyl MethacrylateHCID 11448tert-Butyl methacrylate

Product 1

HCID 18364573HCID 18364573, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

Methyl methacrylate (MM), tert-butyl methacrylate (t-BM) and methacrylic acid (MA) were mixed together with tetrahydrofuran (THF) thereby to obtain a mixed solution, to which 10 mol. % of azoisobutyronitrile (AIBN) was added as an initiator. Then, the resultant mixture was allowed to undergo a reaction for 40 hours to obtain a copolymer (MM-t-BM-MA; 35:30:35) having a molecular weight of 7,000.

Workup

  1. customto obtain a mixed solution
  2. customa reaction for 40 hours

Sources & evidence

ORD record
ord-29c34354ef7f410fbf3b2611fabd1260
Source dataset
uspto-grants-2000_06
Patent number
US06071670

Reaction notes

Loading…