反应详情

Prepared according to Procedure J, using 2-aminobenzoic acid (14.6 g, 106 mmol) and 1-(2-fluorophenyl)propan-1-one (10.78 g, 70.8 mmol) in phosphorous oxychloride (35.00 mL) to afford product as a colorless solid upon purification by chromatography on silica gel, eluting with EtOAc gradient in hexane. Mass Spectrum (ESI) m/e=272.0 (M+1).

1. customPrepared
2. customto afford product as a colorless solid
3. customupon purification by chromatography on silica gel
4. washeluting with EtOAc gradient in hexane