HRID1436025
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
CONDITIONS
反应条件
- 温度
- 50 °C
PROCEDURE
实验过程
Intermediate 4 (25 mg) obtained in Example 6, Step B is added with 10% hydrogen chloride/methanol (10 ml), and the mixture is stirred at 50° C. for 50 hours. The solvent is evaporated under reduced pressure to obtain the title compound as hydrochloride (13 mg (predictive yield)).
WORKUP
后处理
- customThe solvent is evaporated under reduced pressure