4-Nitrobenzaldehyde → HCID 3092129, compound

HRID 1440955Notes

Reaction equation

HRID 1440955 reaction equation
[N+:1]([C:4]1[CH:11]=[CH:10][C:7]([CH:8]=O)=[CH:6][CH:5]=1)([O-:3])=[O:2].Cl.[C:13]1([N:19]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[NH2:20])[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C([O-])(=O)C.[K+].C(O)C>[C:13]1([N:19]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[N:20]=[CH:8][C:7]2[CH:10]=[CH:11][C:4]([N+:1]([O-:3])=[O:2])=[CH:5][CH:6]=2)[CH:14]=[CH:15][CH:16]=[CH:17][CH:18]=1

Participants

5

Reactant 2

HCID 5414-NitrobenzaldehydeHCID 10738Hydrazine, 1,1-diphenyl-, hydrochloride (1:1)

Product 1

HCID 3092129HCID 3092129, compound

Reagents, catalysts & solvents 2

HCID 517044Potassium AcetateCatalystHCID 702EthanolSolvent

Procedure

p-nitrobenzaldehyde and N,N-diphenylhydrazine hydrochloride were heated in the presence of potassium acetate as a catalyst in ethanol to obtain p-nitrobenzaldehyde-N,N-diphenylhydrazone.

Sources & evidence

ORD record
ord-c22eb2d35b134e5787d8818abada3310
Source dataset
uspto-grants-1996_03
Patent number
US05501930

Reaction notes

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