HRID1441387

反应详情

EQUATION

反应方程式

HRID 1441387 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of 0.2 mol of 3-(chloromethyl)tetrahydrofuran, 200 ml of ethanol, 0.2 mol of potassium carbonate and 0.2 mol of ethylenediamine placed in a 500 ml of round-bottomed flask was refluxed for 24 hours, and then the solvent was removed. The obtained product was yellow oily liquid in 77% yield.

WORKUP

后处理

  1. customplaced in a 500 ml of round-bottomed flask
  2. temperaturewas refluxed for 24 hours
  3. customthe solvent was removed