HRID1442879

反应详情

EQUATION

反应方程式

HRID 1442879 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of tert-butyl (2-oxo-3-pyridin-2-ylimidazolidin-1-yl)acetate from Step B (150 mg, 0.54 mmol) in EtOAc (10 mL) at 0° C. was saturated with HCl (g). The mixture was stood at 0° C. for a total of 30 min, then concentrated in vacuo to give the title compound. MS: m/z=222 (M+1).

WORKUP

后处理

  1. customat 0° C.
  2. customwas stood at 0° C. for a total of 30 min
  3. concentrationconcentrated in vacuo