Hydrochloric Acid → HCID 20380293, compound

HRID 1448597Notes

Reaction equation

HRID 1448597 reaction equation
[CH3:1][CH:2]([C:10]1[CH:11]=[C:12]([O:17][CH3:18])[CH:13]=[C:14]([OH:16])[CH:15]=1)[CH:3]([CH3:9])[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[CH3:19][N:20]1[CH2:25][CH2:24][C:23](=O)[CH2:22][CH2:21]1.CCOCC.[ClH:32]>C(O)(=O)C>[ClH:32].[CH3:19][N:20]1[CH2:21][CH:22]=[C:23]([C:13]2[C:12]([O:17][CH3:18])=[CH:11][C:10]([CH:2]([CH3:1])[CH:3]([CH3:9])[CH2:4][CH2:5][CH2:6][CH2:7][CH3:8])=[CH:15][C:14]=2[OH:16])[CH2:24][CH2:25]1

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 740491-Methyl-4-piperidoneHCID 20494745HCID 20494745, compound

Product 1

HCID 20380293HCID 20380293, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

5-(1,2-Dimethylheptyl)-3-methoxyphenol (10.0 g) of Example V, and N-methyl-4-piperidone (4.45 g) were dissolved in 20 ml acetic acid and saturated with HCl gas. Ether was added and the resulting solid recrystallized from isopropyl alcohol-ether. Yield 7.32 g, m.p. 96°-97°.

Workup

  1. customthe resulting solid recrystallized from isopropyl alcohol-ether

Sources & evidence

ORD record
ord-486dc86dbbb1469aae9cfc4b68d0ae9e
Source dataset
uspto-grants-1979_12
Patent number
US04180669

Reaction notes

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