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HRID1449403

反应详情

EQUATION

反应方程式

HRID 1449403 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：FC(F)C(F)(F)Sc1nc(-c2ccccc2)c(-c2ccccc2)[nH]1
HCID13508075

未命名化合物

PRODUCTS

生成物

1
结构：Cl.FC(F)C(F)(F)Sc1nc(-c2ccccc2)c(-c2ccccc2)[nH]1
HCID20349427

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

A solution of 5.0 g of 4,5-diphenyl-2-(1,1,2,2-tetrafluoroethylthio)imidazole (Example 18) in a mixture of ether and tetrahydrofuran was treated with dry hydrogen chloride gas and a precipitate was collected by filtration to give 4.7 g of 4,5-diphenyl-2-(1,1,2,2-tetrafluoroethylthio)imidazole hydrochloride, m.p. 192°-202°.

WORKUP

后处理

  1. filtrationa precipitate was collected by filtration