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HRID1450103

反应详情

EQUATION

反应方程式

HRID 1450103 的结构方程式

REACTANTS

反应物

2
结构：c1ccc(CNCc2ccccc2)cc1
HCID7656

Dibenzylamine

C14H15N

结构：Cc1c(F)nc(F)c(F)c1OC(C)(C)C
HCID10751339

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(F)nc(N(Cc2ccccc2)Cc2ccccc2)c(F)c1OC(C)(C)C
HCID19691352

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

4-t-Butoxy-2,5,6-trifluoro-3-methylpyridine from Step 253c above is reacted with dibenzylamine in ethanol at reflux temperature. Solvent is removed, and the residue is dissolved in methylene chloride and washed with water. The product is purified by column chromatography.

WORKUP

后处理

  1. temperatureat reflux temperature
  2. customSolvent is removed
  3. dissolutionthe residue is dissolved in methylene chloride
  4. washwashed with water
  5. customThe product is purified by column chromatography