HRID1452033

反应详情

EQUATION

反应方程式

HRID 1452033 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

##STR6## 19.2 g of 5,6-dimethoxyindanone, 15 g of pyridine-4-aldehyde and 19 g of p-toluenesulphonic acid were heated to boiling under reflux in a water separator for 5 h in 250 ml of toluene. The resulting precipitate was filtered off with suction after cooling and stirred at room temperature for 30 min in 10% strength sodium carbonate solution. The resulting pale-yellow precipitate was filtered off with suction, washed with water and dried in air. Yield: 24.4 g (87%).

WORKUP

后处理

  1. filtrationThe resulting precipitate was filtered off with suction
  2. temperatureafter cooling
  3. filtrationThe resulting pale-yellow precipitate was filtered off with suction
  4. washwashed with water
  5. customdried in air