HRID1456662

反应详情

EQUATION

反应方程式

HRID 1456662 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of compound 723 (240 mg, 0.53 mmol) in CH2Cl2 (4.0 mL) was added TFA (2.0 mL) and the reaction stirred at rt for 1 hr. The reaction was concentrated in vacuo and the residue co-concentrated with toluene. The material was used directly in the next reaction without further purification. ##STR103##

WORKUP

后处理

  1. concentrationThe reaction was concentrated in vacuo
  2. customThe material was used directly in the next reaction without further purification