HRID1460061

反应详情

EQUATION

反应方程式

HRID 1460061 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Prepared by treatment of 4,6-dichloro-5-nitropyrimidine with N-(2-(benzyloxy)ethyl)benzylamine, followed by reaction with 2ethyl-4-methylimidazole, reduction with fin (II) chloride, cyclization with carbonyldiimidazole, and hydrogenation with palladium on carbon in methanol containing 1.1 eq. NaOH at 50 psi and 50° C. for 24 h.

WORKUP

后处理

  1. customat 50 psi and 50° C.
  2. customfor 24 h.