Diethyl Carbonate → HCID 86745283, compound
Reaction equation
[CH2:1]([OH:19])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[C:20](=O)([O:24]CC)[O:21][CH2:22][CH3:23]>>[C:20](=[O:24])([O:21][CH2:22][CH3:23])[O:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]Participants
3
Procedure
260 g (1 mol) of a technical grade oleyl alcohol were reacted with 118 g (1 mol) of diethyl carbonate in the same way as described under A. The title compound was obtained in a yield of approximately 370 g in the form of a light yellow, clear liquid having an OH value of 8.5, an acid value of 0.1, an iodine value of 76 and a number average molecular weight of 333.
Sources & evidence
- ORD record
- ord-dc643a3e38054b7ea55279ac32aa34ca
- Source dataset
- uspto-grants-1991_12
- Patent number
- US05072015
Reaction notes
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