HRID1462023

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14923

Ammonium hydroxide

H5NO

HCID76727

Morpholine, 4-(2-chloroethyl)-

C6H12ClNO

HCID98086

2-Methyl-1-phenylpiperazine

C11H16N2

PRODUCTS

生成物

HCID20454475

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID887

Methanol

CH4O

2 次

PROCEDURE

实验过程

In the same manner as described in Example 1, N-(2-chloroethyl)morpholine is reacted with 1-phenyl-2-methylpiperazine. The trihydrochloride has a melting point 288°-290° (from methanol); Rf=0.63 (MeOH-conc. NH4OH 97:3); IR (nujol) νmax: 2420, 1500, 1405, 1265, 1060, 770, 695 cm-1 ; 1H-NMR (D2O; (CH3)3Si(CD2)2COONa): 1.05 (d, J=6 Hz; 3H; 2.70-4.20 (m; 19H); 7.47 (s; 5H).