HRID1466016

反应详情

EQUATION

反应方程式

HRID 1466016 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a flask charged with tert-Butyl 4-(6-cyano-1,2,3,4-tetrahydronaphthalen-2-yl)-3-oxopiperazine-1-carboxylate (450 mg, 1.3 mmol) was added 4N HCl in dioxane. The mixture was allowed to stir at RT for 1 hour. LC showed complete reaction. The volatiles were removed under reduced pressure, and the resulting solids were used without further purification. LC-MS (IE, m/z): 256 [M+1]+.

WORKUP

后处理

  1. customreaction
  2. customThe volatiles were removed under reduced pressure
  3. customthe resulting solids were used without further purification