Di-tert-butyl dicarbonate → HCID 68477709, compound

HRID 1466485Notes

Reaction equation

HRID 1466485 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:8](=[C:9]([N+:11]([O-:13])=[O:12])[CH:10]=1)[NH:7][C:6]([C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[CH:5]2.[O:20](C(OC(C)(C)C)=O)[C:21]([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=O>CN(C1C=CN=CC=1)C>[C:21]([N:7]1[C:8]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:10][C:9]=2[N+:11]([O-:13])=[O:12])[CH:5]=[C:6]1[C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)([O:23][C:24]([CH3:27])([CH3:26])[CH3:25])=[O:20]

Participants

4

Reactant 2

HCID 90495Di-tert-butyl dicarbonateHCID 68477399HCID 68477399, compound

Product 1

HCID 68477709HCID 68477709, compound

Reagents, catalysts & solvents 1

HCID 142844-(Dimethylamino)pyridineCatalyst

Procedure

5-Methyl-7-nitro-2-phenyl-1H-indole prepared in Preparation 24, (BOC)2O and DMAP were reacted according to the same procedure as Preparation 23 to give the title compound.

Workup

  1. customwere reacted
  2. customaccording to the same procedure as Preparation 23

Sources & evidence

ORD record
ord-a57c76f8555b474b9a2551e1adf6055b
Source dataset
uspto-grants-2015_04
Patent number
US09000028B2

Reaction notes

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