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HRID1467330

反应详情

EQUATION

反应方程式

HRID 1467330 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)(C)OC(=O)N[C@H]1CCCN(Cc2ccccc2)C1
HCID10541535

(S)-1-Benzyl-3-N-Boc-aminopiperidine

C17H26N2O2

PRODUCTS

生成物

1
结构：N[C@H]1CCCN(Cc2ccccc2)C1
HCID854131

(3S)-1-Benzylpiperidin-3-amine

C12H18N2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

4N HCl in dioxane (1 mL) was added to (S)-tert-butyl 1-benzylpiperidin-3-ylcarbamate (0.5 mmol). The reaction was stirred at room temperature for 30 minutes. The solvent was removed by vacuo. The crude product was progressed to the next step without purification.

WORKUP

后处理

  1. customThe solvent was removed by vacuo
  2. customThe crude product was progressed to the next step without purification