HRID1471001

反应详情

EQUATION

反应方程式

HRID 1471001 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of the compound of Example 120A (2.26 g, 10.00 mmol) in ethyl acetate (35 mL) was treated with 10% palladium on carbon (300 mg) followed by hydrogenation under one atmosphere pressure for 6 h. The mixture was filtered through celite and concentrated in vacuo to afford the title compound as a white solid.

WORKUP

后处理

  1. filtrationThe mixture was filtered through celite and
  2. concentrationconcentrated in vacuo