Hydrochloric Acid → HCID 70980185, compound

HRID 1475398Notes

Reaction equation

HRID 1475398 reaction equation
C(OC([N:8]1[C:16]2[CH:15]=[C:14]([N:17]3[CH2:21][CH2:20][CH2:19][C:18]3=[O:22])[N:13]=[CH:12][C:11]=2[C:10]([CH3:24])([CH3:23])[CH2:9]1)=O)(C)(C)C.[ClH:25]>>[ClH:25].[CH3:23][C:10]1([CH3:24])[C:11]2[CH:12]=[N:13][C:14]([N:17]3[CH2:21][CH2:20][CH2:19][C:18]3=[O:22])=[CH:15][C:16]=2[NH:8][CH2:9]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 70980221HCID 70980221, compound

Product 1

HCID 70980185HCID 70980185, compound

Procedure

3,3-Dimethyl-6-(2-oxo-pyrrolidin-1-yl)-2,3-dihydro-pyrrolo[3,2-c]pyridine-1-carboxylic acid tert-butyl ester (100 mg) was treated with HCl (saturated solution in EtOAc) and stirred for 4 h. The mixture was then evaporated to dryness in vacuo to give the title compound as a pale yellow solid. MS: [M+H]+=232.

Workup

  1. customThe mixture was then evaporated to dryness in vacuo

Sources & evidence

ORD record
ord-e30db00593df461a81d7619318d25573
Source dataset
uspto-grants-2015_04
Patent number
US09018214B2

Reaction notes

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